Abstract: The lead in non-workers blood was determined due to the lead toxicity. Adjacent to the factory exposed in the accumulator production. Method of direct determination of lead Atomic Absorption Spectrophotometry (AAS) . This provide a sensitive and specific method to determine the lead concentration in blood. The procedure precipitated the proteins with trichloroacetic acid (TCA) then the lead extracted with ammonium pyrrolidine dithiocarbonate (APDC) into isobutylmethylketone.